5,5-dimethyl-2-octyl-1,3-dioxane → HCID 178429021, compound

HRID 1490991Notes

Reaction equation

HRID 1490991 reaction equation
CCCCCCCCC1OCC(C)(C)CO1>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCCCCCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc2ccc3cccnc3c2n1.[Ir].[Ir]>CC1(C)COC(CCCCCCCCB2OC(C)(C)C(C)(C)O2)OC1

Participants

6

Reactant 1

HCID 2287815,5-dimethyl-2-octyl-1,3-dioxane

Product 1

HCID 178429021HCID 178429021, compoundYield 47%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 49133562-Methyl-1,10-phenanthrolineReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 9266CyclooctaneSolvent

Conditions

Temperature
100 °C

Sources & evidence

ORD record
ord-2c6b17ddbb764d77a36c39ebe30047bd
Source dataset
Borylation dataset from Roche

Reaction notes

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