HCID 89369290, compound → HCID 178429019, compound

HRID 1490992Notes

Reaction equation

HRID 1490992 reaction equation
CCCCC1(C)OCC(C)(C)CO1>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCCCCCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc2ccc3cccnc3c2n1.[Ir].[Ir]>CC1(C)COC(C)(CCCCB2OC(C)(C)C(C)(C)O2)OC1

Participants

6

Reactant 1

HCID 89369290HCID 89369290, compound

Product 1

HCID 178429019HCID 178429019, compoundYield 54%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 49133562-Methyl-1,10-phenanthrolineReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 9266CyclooctaneSolvent

Conditions

Temperature
100 °C

Sources & evidence

ORD record
ord-b008d25884984d19bc3ef1ee9519b0e7
Source dataset
Borylation dataset from Roche

Reaction notes

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