Cyclohexanol, 1-butyl- → HCID 178431112, compound

HRID 1490997Notes

Reaction equation

HRID 1490997 reaction equation
CCCCC1(O)CCCCC1>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCCCCCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.CC1(C)OBOC1(C)C.C[OH2+].C[OH2+].Cc1ccc2ccc3cccnc3c2n1.[Ir].[Ir]>CC1(C)OB(CCCCC2(O)CCCCC2)OC1(C)C

Participants

7

Reactant 1

HCID 138505Cyclohexanol, 1-butyl-

Product 1

HCID 178431112HCID 178431112, compoundYield 56%

Reagents, catalysts & solvents 5

HCID 2733548Bis(pinacolato)diboraneReagentHCID 27347684,4,5,5-Tetramethyl[1,3,2]dioxaborolaneReagentHCID 49133562-Methyl-1,10-phenanthrolineReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 9266CyclooctaneSolvent

Conditions

Temperature
100 °C

Sources & evidence

ORD record
ord-e83face89a964c0a8cb554dca7e71fd2
Source dataset
Borylation dataset from Roche

Reaction notes

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