6,10-Dioxaspiro[4.5]decane, 8,8-dimethyl- → HCID 172644631, compound

HRID 1491001Notes

Reaction equation

HRID 1491001 reaction equation
CC1(C)COC2(CCCC2)OC1>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCCCCCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc2ccc3cccnc3c2n1.[Ir].[Ir]>CC1(C)COC2(CCC(B3OC(C)(C)C(C)(C)O3)C2)OC1

Participants

6

Reactant 1

HCID 697076,10-Dioxaspiro[4.5]decane, 8,8-dimethyl-

Product 1

HCID 172644631HCID 172644631, compoundYield 31%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 49133562-Methyl-1,10-phenanthrolineReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 9266CyclooctaneSolvent

Conditions

Temperature
100 °C

Sources & evidence

ORD record
ord-d0e3176d5260459a9bc9bfbb8f48e7fe
Source dataset
Borylation dataset from Roche

Reaction notes

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