1-(azepan-1-yl)-2,2,2-trifluoroethanone → HCID 178431061, compound

HRID 1491014Notes

Reaction equation

HRID 1491014 reaction equation
O=C(N1CCCCCC1)C(F)(F)F>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCCCCCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc2ccc3cccnc3c2n1.[Ir].[Ir]>CC1(C)OB(C2CCCCN(C(=O)C(F)(F)F)C2)OC1(C)C

Participants

6

Reactant 1

HCID 45702661-(azepan-1-yl)-2,2,2-trifluoroethanone

Product 1

HCID 178431061HCID 178431061, compoundYield 26%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 49133562-Methyl-1,10-phenanthrolineReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 9266CyclooctaneSolvent

Conditions

Temperature
100 °C

Sources & evidence

ORD record
ord-921d20ade7de4ab88fffeff229935dea
Source dataset
Borylation dataset from Roche

Reaction notes

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