HCID 325024, compound → HCID 178453126, compound

HRID 1491234Notes

Reaction equation

HRID 1491234 reaction equation
CC(C)(C)OC(=O)NC=Cc1ccccc1>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCCCC1.CC(C)(C)c1ccnc(-c2cc(C(C)(C)C)ccn2)c1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].[Ir].[Ir]>CC(C)(C)OC(=O)NC=C(B1OC(C)(C)C(C)(C)O1)c1ccccc1

Participants

6

Reactant 1

HCID 325024HCID 325024, compound

Product 1

HCID 178453126HCID 178453126, compoundYield 73%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 42491874,4'-Di-tert-butyl-2,2'-bipyridylReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 8078CyclohexaneSolvent

Conditions

Temperature
100 °C

Sources & evidence

ORD record
ord-184e49b4eea0492a922839d6894bd517
Source dataset
Borylation dataset from Roche

Reaction notes

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