1,3-Dimethoxybenzene → 2-(3,5-Dimethoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

HRID 1491399Notes

Reaction equation

HRID 1491399 reaction equation
COc1cccc(OC)c1>C1CCc2c(c3c(c4c2CCCC4)CCCC3)C1.CC1(C)OBOC1(C)C.CN1CCCC1=O>COc1cc(OC)cc(B2OC(C)(C)C(C)(C)O2)c1

Participants

5

Reactant 1

HCID 90251,3-Dimethoxybenzene

Product 1

HCID 162176602-(3,5-Dimethoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolaneYield 50%

Reagents, catalysts & solvents 3

HCID 95278DodecahydrotriphenyleneReagentHCID 27347684,4,5,5-Tetramethyl[1,3,2]dioxaborolaneReagentHCID 13387N-methyl-2-pyrrolidoneSolvent

Conditions

Temperature
80 °C

Sources & evidence

ORD record
ord-a96a99e7dec74a9a93ed5d9e77aef1d8
Source dataset
Borylation dataset from Roche

Reaction notes

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