HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1491489Generated: October 25, 2026
HCID 59831133, compound → HCID 101547935, compound
https://huagongshe.com/reaction/1491489
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 59831133 | HCID 59831133 | — |
| Reagent | Bis(pinacolato)diborane | HCID 2733548 | — |
| Reagent | 4,4,5,5-Tetramethyl[1,3,2]dioxaborolane | HCID 2734768 | — |
| Reagent | N,N-Dibenzyl-N'-(pyridin-2-ylmethylene)hydrazine | HCID 67601456 | — |
| Catalyst | Bis(1,5-cyclooctadiene)dimethoxydiiridium | HCID 76001521 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 101547935 | HCID 101547935 | 62% |
Reaction Steps
Following the general procedure, column chromatography (EtOAc/n-hexane 1:6) afforded 9h (141 mg, 62 %) as a yellow viscous oil.
Provenance & Evidence
| DOI | 10.1002/anie.201104544 |
|---|
| Source dataset | Borylation dataset from Roche |
|---|
| ORD ID | ord-622fbdaf489c4efb88e3ef98dbf33ec0 |
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| Source note | Borylation dataset from Roche |
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