HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21459557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Iodide Ion | HCID 30165 | — |
| Reactant | HCID 12040166 | HCID 12040166 | — |
| Reactant | 4,5-Dibromo-2-(trifluoromethyl)-1H-pyrrole-3-carbonitrile | HCID 21459510 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 21459557 | HCID 21459557 | — |
Reaction Steps
3,4,5-Tribromo-pyrrole-2-carbonitrile (1.0 g, 0.003 mo1) is dissolved in a mixture of acetone (20 mL) and dimethoxyethane (10 mL). Potassium carbonate (0.45 g, 0.0033 mol) is added followed by methyl .iodide (0.478 g, 0.0033 mo1). After stirring overnight at room temperature, the mixture is poured into water precipitating a white solid. The solid (0.S g, 80%) has mp 115°-119° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05371239 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-9a8dc11ce05f4874b84311ffd86ebcfa |
| Source note | uspto-grants-1994_12 |