HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 67824007, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Potassium | HCID 5462222 | — |
| Reactant | HCID 14996290 | HCID 14996290 | — |
| Reactant | Methyl 2-[2-(bromomethyl)phenyl]-3-methoxyprop-2-enoate | HCID 53395349 | — |
| Reactant | HCID 54373368 | HCID 54373368 | — |
| Product | HCID 67824007 | HCID 67824007 | 54% |
Reaction Steps
A method similar to Example 3 was used and 6.3 g (32 mmol) of 1-(4-fluorobenzyl)-cyclopropanecarboxylic acid were converted with 2.0 g (36 mmol) of potassium hydroxide into the potassium salt of fluorobenzylcyclopropanecarboxylic acid, and said salt was then reacted at 100° C. with 6.3 g (22 mmol) of methyl alpha-(2-bromomethylphenyl)-beta-methoxyacrylate. Yield: 54%; colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05371268 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-b6c831a1951b46ad915d278c54630782 |
| Source note | uspto-grants-1994_12 |