HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 18952092, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 18952061 | HCID 18952061 | — |
| Product | HCID 18952092 | HCID 18952092 | 41% |
Reaction Steps
Using the procedure described in Example 12, 4-[5-fluoro-3-(3-oxo-2,3-dihydro-4H-1,4-benzothiazin-7-ylthio)phenyl]-4-methoxytetrahydropyran was reacted with methyl iodide to give 4-[5-fluoro-3-(4-methyl-3-oxo-2,3-dihydro-4H-1,4-benzothiazin-7-ylthio)phenyl]-4-methoxytetrahydropyran in 41% yield, m.p. 131°-133° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373007 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-d714861ec3bf423cad56e0dad2369581 |
| Source note | uspto-grants-1994_12 |