HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53720908, compound → [2-(1H-imidazol-1-yl)ethyl]methylamine dihydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53720908 | HCID 53720908 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | [2-(1H-imidazol-1-yl)ethyl]methylamine dihydrochloride | HCID 6483896 | — |
Reaction Steps
The title compound of Step 11 (5.70 g, 26.5 mmol) was reacted with Pd(OH)2 /C in methanol at 60° with 60 psi of hydrogen for 4 hours. Filtration through Celite gave the title compound as a clear, colorless oil (3.46 g). The proton spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373017 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-ee5941b5e5e744adbf1de815787f5871 |
| Source note | uspto-grants-1994_12 |