HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14209946, compound → HCID 14476479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14209946 | HCID 14209946 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14476479 | HCID 14476479 | — |
Reaction Steps
22 g. (0.1 mole) 1,2,3,4-tetrahydro-4,4-dimethyl-6-nitroquinolin-2-one in 500 ml. methanol are, after the addition of 2 g. palladium on charcoal (10%), hydrogenated at atmospheric pressure. After separating off the catalyst, the solvent is removed in a vacuum. Yield 18.4 g. (97% of theory); m.p. 126°-130° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373019 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-6576544c2b5643dea1b093d7a38d5f97 |
| Source note | uspto-grants-1994_12 |