HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 178465569, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | 2-Morpholinoaniline | HCID 735756 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | HCID 178465569 | HCID 178465569 | — |
Reaction Steps
A mixture of 4-(2-aminophenyl)morpholine (5.3 g), acetonitrile (4.52 ml) and anhydrous aluminium chloride (12 g) was heated at 160°-170° C. for 4 hours to yield N-(2-morpholinophenyl)acetamidine (m.p. 140°-141° C.) which was recrystallised from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-ca242a02a8d84b9eb7dce2e6d78885e1 |
| Source note | uspto-grants-1994_12 |