HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 178465572, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 18952141 | HCID 18952141 | — |
| Product | HCID 178465572 | HCID 178465572 | — |
Reaction Steps
A mixture of 4-(2-amino-4-methylphenyl)morpholine (5.76 g), acetonitrile (3.5 g) and anhydrous aluminium chloride (12 g) was heated at 160°-170° C. for 5 hours to yield N-(5-methyl-2-morpholinophenyl)acetamidine (m.p. 121° C.) which was recrystallised from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-d75ce135e40d41ec864e8dbdf53216e0 |
| Source note | uspto-grants-1994_12 |