HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pivalonitrile → HCID 178446834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pivalonitrile | HCID 12416 | — |
| Reactant | 2-Morpholinoaniline | HCID 735756 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | HCID 178446834 | HCID 178446834 | — |
Reaction Steps
A mixture of 4-(2-aminophenyl)morpholine (3.56 g), pivalonitrile (5 g) and anhydrous aluminium chloride (8 g) was heated at 160°-170° C. for six hours to yield N-(2-morpholinophenyl)pivalamidine (m.p. 126° C.) which was recrystallised from hexane and converted into its monofumarate salt (m.p. 211° C.) which was recrystallised from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-68e86047f21b43d3b9078bafb8a10ed1 |
| Source note | uspto-grants-1994_12 |