Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 15746480 | HCID 15746480 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178495928 | HCID 178495928 | — |
Reaction Steps
A mixture of 1-{2-[bis(2-methoxyethyl)amino]phenyl}thiourea (5 g), methyl iodide (1.4 ml) and acetone (25 ml) was heated at 40° C. for 2 hours. Removal of the solvent gave a residue which was triturated with ether to give 2-methyl-1-{2-[bis(2-methoxyethyl)amino]phenyl}-2-thiopseudourea hydroiodide (m.p. 111°-112° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05373008 |
|---|
| Source dataset | uspto-grants-1994_12 |
|---|
| ORD ID | ord-087d4d657a124137b2a097342619ab69 |
|---|
| Source note | uspto-grants-1994_12 |
|---|
