HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178503987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 18952152 | HCID 18952152 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178503987 | HCID 178503987 | — |
Reaction Steps
A mixture of 1-(5-methyl-2-morpholinophenyl)thiourea (14 g), methyl iodide (7.9 g) in methanol (50 ml) was heated at reflux for 2 hours to give 2-methyl-1-(5-methyl-2-morpholinophenyl)-2-thiopseudourea hydroiodide as a pale yellow solid, m.p. 157°-159° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-b7c93cb6acda43b8a31b064147941c23 |
| Source note | uspto-grants-1994_12 |