HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178503986, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 18952310 | HCID 18952310 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178503986 | HCID 178503986 | — |
Reaction Steps
A mixture of 1-(6-methyl-2-piperidinophenyl)thiourea (7 g) and methyl iodide (4.38 g) in dry methanol (100 ml) was heated under reflux for 3 hours to give 2-methyl-1-(6-methyl-2-piperidinophenyl)-2-thiopseudourea hydroiodide as a pale yellow solid, (m.p. 204°-205° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-d9452ef51cdf4608a531e2d8727958ca |
| Source note | uspto-grants-1994_12 |