HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 18952225, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 8625249 | HCID 8625249 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 18952225 | HCID 18952225 | — |
Reaction Steps
A mixture of 1-(2-morpholinophenyl)-3-methylthiourea (5 g) and methyliodide (2.8 g) in acetone (30 ml) was heated at reflux for 4 hours to yield 2-methyl-1-(2-morpholinophenyl)-3-methyl-2-thiopseudourea hydroiodide (m.p. 163°-164° C.) which was recrystallised from a 1:3 mixture of methanol and ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-187a899cb802444aa3eb12b96e9c43da |
| Source note | uspto-grants-1994_12 |