HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 178484905, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 18952225 | HCID 18952225 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178484905 | HCID 178484905 | — |
Reaction Steps
A mixture of 2-methyl-1-(2-morpholinophenyl)-3-methyl-2-thiopseudourea hydroiodide (3.9 g) and 33% methylamine in solution in absolute ethanol (40 ml) was heated for 28 hours at 50°-55° C. to yield 1,3-dimethyl-2-(2-morpholinophenyl)guanidine which was recrystallised from hexane (m.p. 137°-138° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-7d55e7a0d79d460593b1e886c05916cb |
| Source note | uspto-grants-1994_12 |