HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl Isothiocyanate → 1-(n-Butyl)-3-(2-morpholinophenyl)thiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl Isothiocyanate | HCID 11613 | — |
| Reactant | 2-Morpholinoaniline | HCID 735756 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1-(n-Butyl)-3-(2-morpholinophenyl)thiourea | HCID 8625254 | — |
Reaction Steps
A solution of 4-(2-aminophenyl)morpholine (5.8 g) in dichloromethane (60 ml) was treated with n-butyl isothiocyanate (5 g) and mixture stirred at room temperature for 4 days to yield 1-(n-butyl)-3-(2-morpholinophenyl)thiourea as a pale yellow solid (m.p. 105° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-1909c154fd1a48e2a96011edf8172013 |
| Source note | uspto-grants-1994_12 |