HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-(Methylthio)ethyl)amine → HCID 178503813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-(Methylthio)ethyl)amine | HCID 87697 | — |
| Reactant | HCID 178503978 | HCID 178503978 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178503813 | HCID 178503813 | — |
Reaction Steps
A mixture of 2-methyl-1-(2-morpholinophenyl)-2-thiopseudourea hydroiodide (1.7 g) prepared as described in Example 166, 2-methylthioethylamine (1.8 g) and ethanol (25 ml) was heated at 90°-95° C. for 22 hours to give 1-(2-methylthioethyl)-2-(2-morpholinophenyl)guanidine (m.p. 115°-116° C.) which was recrystallised from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-170d2265effa46d3a758d8be2564e12b |
| Source note | uspto-grants-1994_12 |