HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl Isothiocyanate → 1-(n-Butyl)-3-(5-chloro-2-morpholinophenyl)thiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl Isothiocyanate | HCID 11613 | — |
| Reactant | 5-Chloro-2-(morpholin-4-yl)aniline | HCID 846189 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(n-Butyl)-3-(5-chloro-2-morpholinophenyl)thiourea | HCID 18952277 | — |
Reaction Steps
Reaction of 5-chloro-2-morpholinoaniline (2.8 g) (2.8 g) with n-butyl isothiocyanate (1.5 g) in ethanol (20 ml) at room temperature for 60 days yielded 1-(n-butyl)-3-(5-chloro-2-morpholinophenyl)thiourea (m.p. 150°-152° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-7941c82753304f69b45c0214d800a568 |
| Source note | uspto-grants-1994_12 |