HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 18952112, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 15746499 | HCID 15746499 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 18952112 | HCID 18952112 | — |
Reaction Steps
A mixture of 1-methyl-3-[2-(1-pyrrolidinyl)phenyl]thiourea (18.5 g) and methyl iodide (12.3 g) and acetone (100 ml) was heated under reflux for 2.5 hours to give 2-methyl-1-[2-(1-pyrrolidinyl)phenyl]-3-methyl-2-thiopseudourea hydroiodide (m.p. 161°-162° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-74e1f5809c9c41aa84bbe5b8693e3fa9 |
| Source note | uspto-grants-1994_12 |