HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 18952165, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 18952224 | HCID 18952224 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 18952165 | HCID 18952165 | — |
Reaction Steps
A mixture of 1-methyl-3-(5-methyl-2-morpholinophenyl)thiourea (6.4 g) and methyl iodide (3.8 g) in acetone (60 ml) was heated at reflux for 4 hours to give 2-methyl-1-(5-methyl-2-morpholinophenyl)-3-methyl-2-thiopseudourea hydroiodide as a pale yellow solid (m.p. 160°-161° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-7ef48c19716d4b75bfc96073dffe60fb |
| Source note | uspto-grants-1994_12 |