HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → N-(5-chloro-2-morpholinophenyl)cyanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Lead diacetate trihydrate | HCID 22456 | — |
| Reactant | 1-(5-Chloro-2-morpholinophenyl)thiourea | HCID 18952243 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-(5-chloro-2-morpholinophenyl)cyanamide | HCID 18952323 | — |
Reaction Steps
A mixture of 1-(5-chloro-2-morpholinophenyl) thiourea (5.97 g) suspended in water (40 ml), lead acetate trihydrate (8.75 g) in water (40 ml) and potassium hydroxide (12.6 g) in water (35 ml) was heated under reflux for 15 minutes to give N-(5-chloro-2-morpholinophenyl)cyanamide as a white solid (m.p. 305°-308° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-0610919ccddb4761b9f614766bd68ed0 |
| Source note | uspto-grants-1994_12 |