HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 131718012, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 1,1-Dimethyl-2-(2-morpholinophenyl)guanidine | HCID 9885407 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 131718012 | HCID 131718012 | — |
Reaction Steps
Reaction of the product of Example 301 in acetone with concentrated sulphuric acid gave 1,1-dimethyl-2-(2-morpholinophenyl)guanidine hemisulphate (m.p. 234°-235° C.) which was recrystallised from a 1:1 mixture of methanol and ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-b23ad22044614385b40293ab0f64fd63 |
| Source note | uspto-grants-1994_12 |