HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18950654, compound → HCID 178519224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18950654 | HCID 18950654 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178519224 | HCID 178519224 | — |
Reaction Steps
A suspension of 57 g of 3-(pyrid-3-yl)isoxazol-5-one in 50 ml of water and 350 ml of glacial acetic acid is treated dropwise at 15° C. with a solution of 27 g of sodium nitrite in 60 ml of water. After 4 hours, the precipitate is filtered off with suction, washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05374640 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-d1667e8a2bf548ef9e32194f242df821 |
| Source note | uspto-grants-1994_12 |