HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 18951158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-{[(3-Methylphenyl)carbamoyl]amino}acetic acid | HCID 14996960 | — |
| Reactant | HCID 18951128 | HCID 18951128 | — |
| Product | HCID 18951158 | HCID 18951158 | 7.2% |
Reaction Steps
Following a procedure analogous to that described in Example 1, but using 4.8 g of 1-methylcyclopentyl 2-anilinoacetate, 4.1 g of 2-[3-(3-methylphenyl)ureido]acetic acid and 1.4 cm3 of thionyl chloride as starting materials, 0.6 g of 1-methylcyclopentyl 2-{2-[3-(3-methylphenyl)ureido]-N-phenylacetamido}acetate melting at 160° C. is obtained after recrystallization from an acetonitrile/diisopropyl ether mixture (40/60 by volume).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05374656 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-c95d251d70414debb624c5d444e41fcf |
| Source note | uspto-grants-1994_12 |