Hydrochloric Acid → HCID 15232189, compound

Participants

Reaction Steps

To 0.06 g of methyl 4-[2-(4-chlorobenzenesulfonamido)-2-(3-pyridyl)ethyl]phenylacetate in 10 ml of methanol-1,4 dioxane (1:1) solution was added 2 ml of aqueous 2N sodium hydroxide solution, and stirred overnight at room temperature. After completion of reaction, the solution was neutralized with 2 ml of 2N hydrogen chloride. The crystalline deposited was filtered to produce 49 mg of 4-[2-(4-chlorobenzenesulfonamido)-2-(3-pyridyl)ethyl]phenylacetic acid. The spectrometric data thereof supports the structure of [29] as follows.

Provenance & Evidence