HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18950679, compound → HCID 18950677, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18950679 | HCID 18950679 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18950677 | HCID 18950677 | 59% |
Reaction Steps
The N-[2-(4-benzyloxyphenyl)-3-(3-pyridyl)propyl]-4-chlorobenzenesulfonamide (170 mg) was dissolved in 10 ml of ethanol, followed by addition of 0.2 g of 10% palladium carbon, and stirred for catalytic reduction via hydrogen at 55° C. overnight, to obtain 82 mg of N-[2-(4-hydroxyphenyl)-3-(3-pyridyl)propyl]-4-chlorobenzenesulfonamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05374641 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-c503ba70d510426ca868be241eaf36e5 |
| Source note | uspto-grants-1994_12 |