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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1492634Generated: October 31, 2026

Trifluoroacetic acid → HCID 19385695, compound

https://huagongshe.com/reaction/1492634

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 19385639HCID 19385639—
SolventDichloromethaneHCID 6344—
ProductHCID 19385695HCID 1938569557.7%

Reaction Steps

To a solution of 21.4 mg (0.038 mmol) of the product of Step P in CH2Cl2 (1 mL) was added TFA (0.4 mL, 5.19 mmol) at rt. The solution was stirred at rt for 2 hours. The crude mixture was directly purified by flash chromatography eluted with CHCl3 /MeOH/NH4OH (100:10:1) to give 11 mg of the title compound as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05374638
Source datasetuspto-grants-1994_12
ORD IDord-67e426667b6441ce9acf343579e981f7
Source noteuspto-grants-1994_12