Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Fluorophenol | HCID 9732 | — |
| Reactant | 3-Chloropropionyl chloride | HCID 69364 | — |
| Catalyst | Triethylamine | HCID 8471 | — |
| Product | HCID 14069823 | HCID 14069823 | 97.8% |
Reaction Steps
3-Chloropropionyl chloride (391.5 g) and 3 drops of triethylamine is added to 4-fluorophenol (308.3 g) under stirring at 60° C. After heating to 100° C. for 1.5 hrs, distillation gives 544.7 g of (I) boiling at 126°-130° C. 10 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05376687 |
|---|
| Source dataset | uspto-grants-1994_12 |
|---|
| ORD ID | ord-e56a908b6fb042ee8a5b9bffe6ca680a |
|---|
| Source note | uspto-grants-1994_12 |
|---|
