反应详情

温度

60 °C

3-Chloropropionyl chloride (391.5 g) and 3 drops of triethylamine is added to 4-fluorophenol (308.3 g) under stirring at 60° C. After heating to 100° C. for 1.5 hrs, distillation gives 544.7 g of (I) boiling at 126°-130° C. 10 mm Hg.

1. temperatureAfter heating to 100° C. for 1.5 hrs
2. distillationdistillation