HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178479330, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 4-Chloroaniline hydrochloride | HCID 5284363 | — |
| Reactant | HCID 178512369 | HCID 178512369 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178479330 | HCID 178479330 | 130.2% |
Reaction Steps
To 20 g of N1 -cyano-N3 -(3,4-dichlorobenzyl)-guanidine and 13.5 g of 4-chloroaniline hydrochloride, 200 ml of water was added, which was heated and refluxed for 2 hours. When cooled gradually after reaction, crystals was precipiated. After filtering the crystals, by drying the crystals obtained by heat treatment in 200 ml of ethyl acetate, 21.8 g of the captioned compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05376686 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-a5a508994e1b4bf1b9d42cae9f016248 |
| Source note | uspto-grants-1994_12 |