HRID1493116
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
1.02 Grams of calcium (II) methoxide (0.01 mol) was weighed in a round bottom flask in a dry box. A mixture of 0.875 g of (0.01 mol) of methacrylic acid and 2.930 g (0.01 mol) of oleic acid was mixed in 19 g of dry tetrahydrofuran. This acid-mixture was introduced into a round bottom flask which was purged with argon. The contents were magnetically stirred overnight (20 hr) at ambient temperature. The volatile matter was then removed in vacuo (0.1 mm Hg) for 10 hours at room temperature. The resulting solid was analyzed for its metal content.
WORKUP
后处理
- additionThis acid-mixture was introduced into a round bottom flask which
- customwas purged with argon
- custom(20 hr)
- customat ambient temperature
- customThe volatile matter was then removed in vacuo (0.1 mm Hg) for 10 hours at room temperature