HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethyl-1H-pyrazole-1-carboxamidine mononitrate → HCID 178483216, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethyl-1H-pyrazole-1-carboxamidine mononitrate | HCID 198186 | — |
| Reactant | 3-(3-Aminopropoxy)-N,N-dimethylbenzenemethanamine | HCID 12913950 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178483216 | HCID 178483216 | 50.9% |
Reaction Steps
3-(3-Aminopropoxy)-N,N-dimethylbenzenemethanamine (2 g) and 3,5-dimethylpyrazole-1-carboxamidine nitrate (2.1 g) were heated at reflux in ethanol for 16 hr. The solvent was removed and the residue was washed with boiling ethyl acetate before it was crystallised from ethanol to give the title compound as a white solid (1 g) m.p. 123°-4°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05021429 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-888418036a134e4399e439f40c7cec00 |
| Source note | uspto-grants-1991_06 |