HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 12816954, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | 3-(3-Aminopropoxy)-N,N-dimethylbenzenemethanamine | HCID 12913950 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 12816954 | HCID 12816954 | — |
Reaction Steps
Methyl isocyanate (0.27 ml) and 3-(3-aminopropoxy)-N,N-dimethylbenzenemethanamine (0.97 g) were stirred at room temperature in acetonitrile for 2 hours. The title compound was filtered off, washed with acetonitrile and recrystallised from ethyl acetate as colourless prisms (0.49 g) m.p. 79.5°-80°. TLC silica; methanol:0.88 ammonia (80:1) Rf 0.45.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05021429 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-e03fe7b5d25f432f998399aa523ef35f |
| Source note | uspto-grants-1991_06 |