HRID1493209

反应详情

EQUATION

反应方程式

HRID 1493209 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2.1 g of 4-pentafluoroethylbenzyl isothiocyanate and 0.78 g of 2,2,2-trifluoroethylamine were dissolved in 20 ml of ethyl acetate, and the solution was left to stand at room temperature for 24 hours. Ethyl acetate was evaporated under reduced pressure. The resulting white crystals were recrystallized from hexane to give 2.6 g of the captioned compound.

WORKUP

后处理

  1. waitthe solution was left
  2. customEthyl acetate was evaporated under reduced pressure
  3. customThe resulting white crystals were recrystallized from hexane