Triphenylphosphine → HCID 19831262, compound

Participants

Reaction Steps

A stirred solution of 1-bromo-10,10,10-trifluorodecane (4.75 g) and triphenylphosphine (4.53 g) in acetonitrile (100 ml) was heated under reflux for 3 days. The solution was evaporated under vacuum and the residue was washed with ether, dissolved in toluene and the solution diluted with ether to give the product as a hygroscopic solid.

Provenance & Evidence