HCID 178523901, compound → HCID 178512136, compound

HRID 1493345Notes

Reaction equation

HRID 1493345 reaction equation
C([NH:9][C:10]([NH:21][CH2:22][CH2:23][CH2:24][C:25]1[N:26]=[CH:27][NH:28][CH:29]=1)=[N:11][CH2:12][CH2:13][CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)(=O)C1C=CC=CC=1>Cl>[NH:28]1[CH:29]=[C:25]([CH2:24][CH2:23][CH2:22][NH:21][C:10]([NH:11][CH2:12][CH2:13][CH2:14][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[NH:9])[N:26]=[CH:27]1

Participants

3

Reactant 1

HCID 178523901HCID 178523901, compound

Product 1

HCID 178512136HCID 178512136, compound

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Procedure

0.73 g (1.9 mmol) of N-benzoyl-N'-[(3-imidazol-4-yl) propyl]-N"-(3-phenylpropyl)-guanidine are heated under reflux in 45 ml of 20% hydrochloric acid for 7 hours. The method of working up is analogous to that of Example 58.

Sources & evidence

ORD record
ord-311bdf262ae54c69af785cb66427198f
Source dataset
uspto-grants-1991_06
Patent number
US05021431

Reaction notes

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