HCID 178523900, compound → HCID 178512139, compound

HRID 1493346Notes

Reaction equation

HRID 1493346 reaction equation
C([NH:9][C:10]([NH:27][CH2:28][CH2:29][CH2:30][C:31]1[N:32]=[CH:33][NH:34][CH:35]=1)=[N:11][CH2:12][CH2:13][CH:14]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)(=O)C1C=CC=CC=1>Cl>[NH:34]1[CH:35]=[C:31]([CH2:30][CH2:29][CH2:28][NH:27][C:10]([NH:11][CH2:12][CH2:13][CH:14]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[NH:9])[N:32]=[CH:33]1

Participants

3

Reactant 1

HCID 178523900HCID 178523900, compound

Product 1

HCID 178512139HCID 178512139, compound

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Procedure

0.84 g (1.8 mmol) of N-benzoyl-N'-[3-(imidazol-4-yl) propyl]-N"-(3,3-diphenylpropyl)-guanidine are heated under reflux in 45 ml of 20% hydrochloric acid for 7 hours. The method of working up is analogous to that of Example 58.

Sources & evidence

ORD record
ord-fcf09c93116c4765ae587dbde06dfb2b
Source dataset
uspto-grants-1991_06
Patent number
US05021431

Reaction notes

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