HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 19768373, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 2,2,6,6-Tetramethyl-1-(1-phenylethoxy)piperidin-4-one | HCID 17968359 | — |
| Solvent | Toluene | HCID 1140 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 19768373 | HCID 19768373 | 74% |
Reaction Steps
The title compound is prepared in 74% yield as a colorless syrup from n-butylamine and 1-alpha-methylbenzyloxy-2, 2,6,6-tetramethylpiperidin-4-one (made in Example 11A) according to the procedure of Example 11B. Acetonitrile is substituted for tetrahydrofuran as the reaction solvent and toluene is substituted for ether in the isolation steps.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05021481 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-236d4919ed3c4ee795f2d851af292112 |
| Source note | uspto-grants-1991_06 |