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HRID1493448

反应详情

EQUATION

反应方程式

HRID 1493448 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)OCC(CO)O1
HCID7528

Solketal

C6H12O3

结构：O=C1OC(=O)[C@H](Cc2ccccc2)C[C@H]1Cc1ccccc1
HCID14557658

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)OCC(COC(=O)[C@H](Cc2ccccc2)C[C@@H](Cc2ccccc2)C(=O)O)O1
HCID14997152

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

A solution of 1.0 g of (S,S)-2,4-dibenzylglutaric anhydride and 0.54 g of 4-hydroxymethyl-2,2-dimethyl-1,3-dioxolane in 10 ml of toluene is refluxed overnight. The solution is washed with water, dried (Na2SO4), filtered and concentrated to give 4-[(2,2-dimethyl-1,3-dioxolan-4-yl)-methoxycarbonyl]-(S,S)-2,4-dibenzylbutyric acid as a viscous oil.

WORKUP

后处理

  1. washThe solution is washed with water
  2. dry with materialdried (Na2SO4)
  3. filtrationfiltered
  4. concentrationconcentrated