HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54691271, compound → HCID 11989638, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54691271 | HCID 54691271 | — |
| Solvent | Hydrogen Bromide | HCID 260 | — |
| Product | HCID 11989638 | HCID 11989638 | 82.8% |
Reaction Steps
In 640 ml of 47% hydrobromic acid was suspended 8.0 g of 4-hydroxy-7-methoxy-3-(2-methoxyphenyl)-2quinolone, and the suspension was heated under reflux for 3-4 days. After cooling, the precipitates were collected by filtration, washed with water, and dried to obtain 5.6 g of 3-hydroxy-5H-benzofuro[3,2-c]quinolin-6-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05023261 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-a161cf8d366d456ab7ded4d793295a62 |
| Source note | uspto-grants-1991_06 |