HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → 1-[(4-Methoxyphenyl)Methoxy]-3-nitro-Benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | 3-Nitrophenol | HCID 11137 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 1-[(4-Methoxyphenyl)Methoxy]-3-nitro-Benzene | HCID 3628388 | — |
Reaction Steps
A mixture of 3-nitrophenol (18.49 g, 0.133 mol), anhydrous potassium carbonate (19.2 g, 0.139 mol), potassium iodide (21.0 g, 0.127 mol) and 4-methoxybenzyl chloride (19.82 g, 0.127 mol) in acetone (200 ml) was heated under reflux for 48 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05023255 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-837abdd7a1da4fada29afe4bd91f6281 |
| Source note | uspto-grants-1991_06 |