HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acrylate → HCID 11206303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Diethanolamine | HCID 8113 | — |
| Product | HCID 11206303 | HCID 11206303 | — |
Reaction Steps
A mixture of 10.5 grams of diethanolamine and 17.2 grams of methyl acrylate is heated under reflux for 24 hours. The excess methyl acrylate is removed under reduced pressure and the residue is purified using flash chromatography to afford the title compound as a thick oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05023283 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-984b97fc8d6f4b67b34e64d9d88adcb4 |
| Source note | uspto-grants-1991_06 |