Methyl Acrylate → HCID 11206303, compound

HRID 1493659Notes

Reaction equation

HRID 1493659 reaction equation
[NH:1]([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4].[C:8]([O:12][CH3:13])(=[O:11])[CH:9]=[CH2:10]>>[CH3:13][O:12][C:8]([CH2:9][CH2:10][N:1]([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4])=[O:11]

Participants

3

Reactant 2

HCID 7294Methyl AcrylateHCID 8113Diethanolamine

Product 1

HCID 11206303HCID 11206303, compound

Procedure

A mixture of 10.5 grams of diethanolamine and 17.2 grams of methyl acrylate is heated under reflux for 24 hours. The excess methyl acrylate is removed under reduced pressure and the residue is purified using flash chromatography to afford the title compound as a thick oil.

Workup

  1. temperatureis heated
  2. temperatureunder reflux for 24 hours
  3. customThe excess methyl acrylate is removed under reduced pressure
  4. customthe residue is purified

Sources & evidence

ORD record
ord-984b97fc8d6f4b67b34e64d9d88adcb4
Source dataset
uspto-grants-1991_06
Patent number
US05023283

Reaction notes

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