Phenoxyacetic Acid → HCID 86744749, compound

Participants

Reaction Steps

A mixture of 8.2 gm (0.04 mole) of butyric acid [1-4-pyridinyl)ethylidene]hydrazide (Compound 144), 6.09 gm (0.04 mole) of phenoxyacetic acid and 100 ml of absolute ethanol is refluxed 7.5 hr. The reaction mixture is evaporated to dryness in vacuo. The solid is crystallized from ethanol to yield 9.48 gm (66%) of the title compound having a melting point of 105.8° C.

Provenance & Evidence